In-operando XRD on a pouch cell
Demonstration of how to setup operando XRD experiments on full batteries.
Get an insight into how your battery cell behaves under real operating conditions. Investigate coin, electrochemical, pouch, and prismatic cells with in-situ charge-discharge cycling.
Demonstration of how to setup operando XRD experiments on full batteries.
With full integration of potentiostat and environment chambers, Empyrean XRD has extensive in-operando capabilities to investigate the changes occurring in cathode and anode materials as the cell is charged and discharged. Flexibility in X-ray source, optics, and detectors make the Empyrean able to investigate a wide range of battery cells. With recently added Variable Temperature Electrochemical Cells (VTEC and VTEC-trans), take your battery research to new levels by understanding how the cell behaves at low and high real operating conditions, or how solid-state electrolyte battery chemistry felicitates ionic transport at elevated temperatures.
CR20xx coin cells with one or two sided Kapton window can be mounted for in-operando cycling on Empyrean or Aeris XRD, and can be analysed in reflection or transmission mode.
Assemble half or full cell of any battery chemistry in our proprietary variable temperature electrochemical cell and investigate in-operando and in-situ over -10 to 70 Deg temperature range.
Investigate pouch cell in-operando and in-situ over -10 to 70 Deg temperature range with fully integrated VTEC-Trans.
With the 3rd generation Empyrean, Malvern Panalytical has now redefined the concept of a multipurpose diffractometer: the newly designed MultiCore Optics enable the largest variety of measurements without any manual intervention. Empyrean has the unique ability to measure all sample types - from powders to coatings, from nanomaterials to solid objects - on a single instrument…
The operando (operating) technique enables real-time X-ray diffraction (XRD) characterization of crystalline and amorphous phases in battery materials, including electrodes. The structural evolution of phases can be tracked during the charge-discharge cycling of the battery. The ion-exchange reaction can be studied under varying operating conditions for a deeper understanding of battery performance, stability and lifetime.
The research neutron source Heinz Maier-Leibnitz (FRM II) is a central scientific institute of the Technical University of Munich (TUM). The cooperation between the TUM, Forschungszentrum Jülich and Helmholtz Zentrum Geesthacht (HZG), with the collaboration of the Max Planck Society and nine further University groups, is known as the “Heinz Maier-Leibnitz Zentrum” (MLZ). Various working groups of the cooperation partners of the MLZ are conducting research in various fields of which materials science is one.
This customer conducted an analysis of cathode materials for advanced Li-ion batteries and next-generation battery systems with XRD System 'Empyrean'.